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afm:safety_and_lab_regulations [2017/01/12 15:25] – [Inorganic chemicals] galliafm:safety_and_lab_regulations [2023/11/22 15:58] (current) – [High voltages] galli
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   * Rule number ZERO is: if you don't know, ASK. Failing to ask something critical may result in expensive equipment damage but also waist your time.   * Rule number ZERO is: if you don't know, ASK. Failing to ask something critical may result in expensive equipment damage but also waist your time.
   * Scanning Probe Techniques are sensitive to acoustic and mechanical vibrations: do not shout loud, do not make excessive noise, do not jump and smash doors in the SPM Lab.   * Scanning Probe Techniques are sensitive to acoustic and mechanical vibrations: do not shout loud, do not make excessive noise, do not jump and smash doors in the SPM Lab.
-  * Scanning Probe Microscopes (all the parts, heads, tip, sample mounts etc) are sensitive to dirt, organic and powder contamination. Try to use POWDER FREE GLOVES as much as possible when handling all these parts, including when mounting sample and tip.+  * Scanning Probe Microscopes (all the parts, heads, tip, sample mounts etc) are sensitive to dirt, organic and powder contamination. Try to use POWDER FREE GLOVES as much as possible when handling all these parts, including when mounting sample and tip. Or otherwise clean your hands well before using the equipment.
   * Keep the lab tables tidy and clean!   * Keep the lab tables tidy and clean!
-  * Fill in the common LOGBOOK EVERY TIME you measure. +  * Fill in the common LOGBOOK (electronic sheet on the desktop) EVERY TIME you measure. 
   * You experience a problem with a setup? Contact laboratory staff asap.   * You experience a problem with a setup? Contact laboratory staff asap.
   * You see that some stock (tips, gloves, tissues etc) is running out? Order new a.s.a.p. or [[afm:about|ask someone to do it]] for you.   * You see that some stock (tips, gloves, tissues etc) is running out? Order new a.s.a.p. or [[afm:about|ask someone to do it]] for you.
-  * Done with a measurement? Retract the tip, set X,Y,Z high voltage to ZERO (Scan size, Offsets=0) at the Door AFM. Remove sample and tip holder. Close the door of the sound box. +  * Done with a measurement? Remove sample and tip holder. Close the door of the sound box. 
   * Remove all your sample boxes and basic tools from the tables of the SPM Lab when you are done with your measurements.   * Remove all your sample boxes and basic tools from the tables of the SPM Lab when you are done with your measurements.
-  * If you use the SPM Lab regularly, you are supposed to attend the SPM Lab user meetings (announced by email) on regular basis.  
   * SPM lab staff will NOT make regular backups of your data - we only backup the operating systems.   * SPM lab staff will NOT make regular backups of your data - we only backup the operating systems.
   * Users are obliged to acknowledge the SPM Lab in the publications with the following sentence: "AFM measurements were performed in the AFM Facility of the Leiden Institute of Physics (LION)"   * Users are obliged to acknowledge the SPM Lab in the publications with the following sentence: "AFM measurements were performed in the AFM Facility of the Leiden Institute of Physics (LION)"
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 +===== Biological samples =====
  
 +Some biological samples (like human tissues) require special procedures. The LION SPM Lab is NOT a MLx laboratory! It is not allowed to bring biological hazards in the AFM lab.
  
 +There are procedures that can enable you to carry out experiments on biological samples/human tissues in the SPM Lab in a proper and non-dangerous way. You are obliged to contact laboratory staff (<galli@physics.leidenuniv.nl>) before carrying out experiments on biological samples. We can instruct you on how to perform your experiments safely.
  
  
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 It is NOT ALLOWED to use chemicals in the SPM Lab apart from the provided ethanol, acetone, isopropyl alchool and demi-water.\\ It is NOT ALLOWED to use chemicals in the SPM Lab apart from the provided ethanol, acetone, isopropyl alchool and demi-water.\\
  
-Extensive sample preparations should NOT take place in the SPM Lab.\\+Extensive sample preparations should NOT take place in the SPM Lab. We have both clean room and chemical labs close by. Please contact laboratory staff for their use.\\
  
  
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 ===== High voltages ===== ===== High voltages =====
 Many systems work with very high voltages, and in some cases HV power supplies can deliver significant current (several amps). Many systems work with very high voltages, and in some cases HV power supplies can deliver significant current (several amps).
-The systems are equipped with protection circuits but these can never cover all possibilities, so when you disconnect power supply cables to connect them to a different sputtering source for example or when you open vacuum systems be //very careful// that the mains are switched off.+ 
 +Never open the electrical equipment in use in the AFM Lab. This is done exclusively by the lab manager.
  
 Also be careful with water leaks in electrical systems and with jewelery (a necklace can dangle through the ventilation slits of an electric box and is therefore not allowed). Also be careful with water leaks in electrical systems and with jewelery (a necklace can dangle through the ventilation slits of an electric box and is therefore not allowed).
 +
 +If you are planning to use electrical equipment with the microscopes that is not available already in the lab, this should be either CE certified or built in our Electronic Department.
afm/safety_and_lab_regulations.1484234735.txt.gz · Last modified: 2017/01/12 15:25 by galli

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